<?xml version="1.0" encoding="UTF-8"?>
<!DOCTYPE root>
<article xmlns:mml="http://www.w3.org/1998/Math/MathML" xmlns:xlink="http://www.w3.org/1999/xlink" xmlns:xsi="http://www.w3.org/2001/XMLSchema-instance" xmlns:ali="http://www.niso.org/schemas/ali/1.0/" article-type="research-article" dtd-version="1.2" xml:lang="en"><front><journal-meta><journal-id journal-id-type="publisher-id">Analitika</journal-id><journal-title-group><journal-title xml:lang="en">Analitika</journal-title><trans-title-group xml:lang="ru"><trans-title>Аналитика</trans-title></trans-title-group></journal-title-group><issn publication-format="print">2227-572X</issn><issn publication-format="electronic">2687-1351</issn><publisher><publisher-name xml:lang="en">Technosphera JSC</publisher-name></publisher></journal-meta><article-meta><article-id pub-id-type="publisher-id">629021</article-id><article-id pub-id-type="doi">10.22184/2227-572X.2023.13.2.94.104</article-id><article-categories><subj-group subj-group-type="toc-heading"><subject>Аналитика веществ и материалов</subject></subj-group><subj-group subj-group-type="article-type"><subject>Research Article</subject></subj-group></article-categories><title-group><article-title xml:lang="en">Nanoscale Materials in Analytical Atomic Spectrometry</article-title><trans-title-group xml:lang="ru"><trans-title>Наноразмерные материалы в аналитической атомной спектрометрии</trans-title></trans-title-group></title-group><contrib-group><contrib contrib-type="author"><name-alternatives><name xml:lang="en"><surname>Kubrakova</surname><given-names>I. V.</given-names></name><name xml:lang="ru"><surname>Кубракова</surname><given-names>И. В.</given-names></name></name-alternatives><address><country country="RU">Russian Federation</country></address><bio xml:lang="ru"><p>д. х. н.</p></bio><email>kubrakova@geokhi.ru</email><xref ref-type="aff" rid="aff1"/></contrib><contrib contrib-type="author"><name-alternatives><name xml:lang="en"><surname>Prjazhnikov</surname><given-names>D. V.</given-names></name><name xml:lang="ru"><surname>Пряжников</surname><given-names>Д. В.</given-names></name></name-alternatives><address><country country="RU">Russian Federation</country></address><bio xml:lang="ru"><p>к. х. н.</p></bio><email>kubrakova@geokhi.ru</email><xref ref-type="aff" rid="aff1"/></contrib><contrib contrib-type="author"><name-alternatives><name xml:lang="en"><surname>Tjutjunnik</surname><given-names>O. N.</given-names></name><name xml:lang="ru"><surname>Тютюнник</surname><given-names>О. Н.</given-names></name></name-alternatives><address><country country="RU">Russian Federation</country></address><bio xml:lang="ru"><p>к. х. н.</p></bio><email>kubrakova@geokhi.ru</email><xref ref-type="aff" rid="aff1"/></contrib><contrib contrib-type="author"><name-alternatives><name xml:lang="en"><surname>Kiseleva</surname><given-names>M. S.</given-names></name><name xml:lang="ru"><surname>Киселева</surname><given-names>М. С.</given-names></name></name-alternatives><address><country country="RU">Russian Federation</country></address><bio xml:lang="ru"><p>к. х. н.</p></bio><email>kubrakova@geokhi.ru</email><xref ref-type="aff" rid="aff1"/></contrib><contrib contrib-type="author"><name-alternatives><name xml:lang="en"><surname>Efanova</surname><given-names>O. O.</given-names></name><name xml:lang="ru"><surname>Ефанова</surname><given-names>О. О.</given-names></name></name-alternatives><address><country country="RU">Russian Federation</country></address><email>kubrakova@geokhi.ru</email><xref ref-type="aff" rid="aff1"/></contrib></contrib-group><aff-alternatives id="aff1"><aff><institution xml:lang="en"></institution></aff><aff><institution xml:lang="ru">Институт геохимии и аналитической химии им. В. И. Вернадского РАН (ГЕОХИ РАН)</institution></aff></aff-alternatives><pub-date date-type="pub" iso-8601-date="2023-03-11" publication-format="electronic"><day>11</day><month>03</month><year>2023</year></pub-date><volume>13</volume><issue>2</issue><issue-title xml:lang="en"/><issue-title xml:lang="ru"/><fpage>94</fpage><lpage>105</lpage><history><date date-type="received" iso-8601-date="2024-03-12"><day>12</day><month>03</month><year>2024</year></date><date date-type="accepted" iso-8601-date="2024-03-12"><day>12</day><month>03</month><year>2024</year></date></history><permissions><copyright-statement xml:lang="en">Copyright ©; 2023, Kubrakova I.V., Prjazhnikov D.V., Tjutjunnik O.N., Kiseleva M.S., Efanova O.O.</copyright-statement><copyright-statement xml:lang="ru">Copyright ©; 2023, Кубракова И.В., Пряжников Д.В., Тютюнник О.Н., Киселева М.С., Ефанова О.О.</copyright-statement><copyright-year>2023</copyright-year><copyright-holder xml:lang="en">Kubrakova I.V., Prjazhnikov D.V., Tjutjunnik O.N., Kiseleva M.S., Efanova O.O.</copyright-holder><copyright-holder xml:lang="ru">Кубракова И.В., Пряжников Д.В., Тютюнник О.Н., Киселева М.С., Ефанова О.О.</copyright-holder></permissions><self-uri xlink:href="https://journals.eco-vector.com/2227-572X/article/view/629021">https://journals.eco-vector.com/2227-572X/article/view/629021</self-uri><abstract xml:lang="en"><p>The variety of properties of highly dispersed 3nano4 materials made them promising for use in inorganic analysis, including atomic spectrometry 3atomic absorption spectrometry, atomic emission and mass spectrometry with inductively coupled plasma4. These materials are used as solid&gt; phase extractants and matrix modifiers, and are also the object of analysis. The article discusses ways to obtain and characterize nanoparticles; provides data on the structure and properties of magnetic nanoparticles, intended for solving analytical and biomedical problems; shows the possibility of increasing thesensitivity and selectivity of the determination of a:number of elements using nanoparticles in atomic absorption spectrometry with electrothermal atomization and in the cold vapor technique. The new possibilities of spectrometric methods for bioanalytical applications involving nanopar ticles, including inductively coupled plasma mass spectrometry in the single particle mode, are analyzed.</p></abstract><trans-abstract xml:lang="ru"><p>Разнообразие свойств высокодисперсных (нано) материалов обусловило перспективность их использования в неорганическом анализе, включая атомную спектрометрию (атомно-абсорбционная спектрометрия, атомно-эмиссионная и масс-спектрометрия с индуктивно связанной плазмой). Эти материалы применяются в качестве твердофазных экстрагентов и матричных модификаторов, а также являются объектами анализа.</p> <p>В статье рассмотрены пути получения и характеризации наночастиц; приведены данные о структуре и свойствах магнитных наночастиц, предназначенных для решения аналитических и биомедицинских задач; показана возможность повышения чувствительности и селективности определения ряда элементов при использовании наночастиц в атомно-абсорбционной спектрометрии с электротермической атомизацией и в методе холодного пара. Проанализированы новые возможности спектрометрических методов для биоаналитических приложений с участием наночастиц, включая масс-спектрометрию с индуктивно связанной плазмой в режиме единичных частиц.</p></trans-abstract><kwd-group xml:lang="en"><kwd>methods of atomic spectrometry DETAAS</kwd><kwd>AESFICP</kwd><kwd>MSFICPG</kwd><kwd>nanosized materials</kwd><kwd>solidF phase extractants</kwd><kwd>matrix modifiers</kwd><kwd>bioanalysis</kwd></kwd-group><kwd-group xml:lang="ru"><kwd>методы атомной спектрометрии (ЭТААС, АЭС-ИСП, МС-ИСП)</kwd><kwd>наноразмерные материалы</kwd><kwd>твердофазные экстрагенты</kwd><kwd>матричные модификаторы</kwd><kwd>биоанализ</kwd></kwd-group><funding-group/></article-meta></front><body></body><back><ref-list><ref id="B1"><label>1.</label><mixed-citation>Кубракова И. В., Пряжников Д. В. Микроволновый синтез наноразмерных магнитных сорбентов. Журнал аналитической химии. 2021. 76(1):20.</mixed-citation></ref><ref id="B2"><label>2.</label><mixed-citation>Kubrakova I. V., Pryazhnikov D. V. Microwave-assisted synthesis of nanosized magnetic adsorbents. Journal of Analytical Chemistry. 2021. 76(1):15.</mixed-citation></ref><ref id="B3"><label>3.</label><mixed-citation>Пряжников Д. В., Кубракова И. В. Магнитные наноразмерные материалы с модифицированной поверхностью: получение и исследование структуры, состава и свойств. Журнал аналитической химии. 2021. 76(6):496.</mixed-citation></ref><ref id="B4"><label>4.</label><mixed-citation>Pryazhnikov D. V., Kubrakova I. V. Surface-modified magnetic nanoscale materials: preparation and study of their structure, composition, and properties. Journal of Analytical Chemistry. 2021. 76(6):685.</mixed-citation></ref><ref id="B5"><label>5.</label><mixed-citation>Pryazhnikov D. V., Kubrakova I. V., Kiseleva M. S. et al. Preparation and structural characterization of nanosized magnetic solid-phase extractants. Mendeleev Commun. 2014. 24(2):130.</mixed-citation></ref><ref id="B6"><label>6.</label><mixed-citation>Warner C. L., Addleman R.Sh., Cinson A. D., Droubay T. C., Engelhard M. H., Nash M. A., Yantasee W., Warner M. G. High-Performance, Superparamagnetic, Nanoparticle Based Heavy Metal Sorbents for Removal of Contaminants from Natural Waters. ChemSusChem. 2010. 3:749.</mixed-citation></ref><ref id="B7"><label>7.</label><mixed-citation>Киселева М. С., Пряжников Д. В., Кубракова И. В. Магнитный сорбент с мезопористой оболочкой для одновременного концентрирования экотоксикантов различной природы. Журнал аналитической химии. 2018. 73(1):14–21.</mixed-citation></ref><ref id="B8"><label>8.</label><mixed-citation>Kiseleva M. S., Pryazhnikov D. V., Kubrakova I. V. Magnetic sorbent with a mesoporous shell for the simultaneous preconcentration of ecotoxicants of different nature. Journal of Analytical Chemistry. 2018. 73(1):10.</mixed-citation></ref><ref id="B9"><label>9.</label><mixed-citation>Zou Z., Hu J., Xu F., Hou X., Jiang X. Nanomaterials for photochemical vapor generation-analytical atomic spectrometry. Trends in Analytical Chemistry. 2019. 114:242.</mixed-citation></ref><ref id="B10"><label>10.</label><mixed-citation>Sturgeon R. E. and Grinberg P. Some speculations on the mechanisms of photochemical vapor generation. J. Anal. At. Spectrom. 2012. 27:222.</mixed-citation></ref><ref id="B11"><label>11.</label><mixed-citation>Zou Z., Jiang X., Li L., Yao Q., Luo H., Huang K. Photochemical vapor generation of selenium: Mechanisms and applications. Trends in Environmental Analytical Chemistry. 2020. 27.</mixed-citation></ref><ref id="B12"><label>12.</label><mixed-citation>He C., Cheng G., Zheng C., Wu L., Lee Y., Hou X. Photochemical vapor generation and in situ preconcentration for determination of mercury by graphite furnace atomic absorption spectrometry. Anal. Methods. 2015. 7:3015.</mixed-citation></ref><ref id="B13"><label>13.</label><mixed-citation>Volynsky A. B., Krivan V. Comparison of various forms of palladium used as chemical modifiers for the determination of selenium by electrothermal atomic absorption spectrometry. Journal of Analytical Atomic Spectrometry. 1996. 11:159.</mixed-citation></ref><ref id="B14"><label>14.</label><mixed-citation>Zangmo T., Siripinyanond A. Exploring the applicability of nano-selenium for capture of mercury vapor: Paper based sorbent and a chemical modifier in graphite furnace atomic absorption spectrometry. Analyt. Chim. Acta. 2019. 1085.</mixed-citation></ref><ref id="B15"><label>15.</label><mixed-citation>Пряжников Д. В., Ефанова О. О., Киселева М. С., Кубракова И. В. Микроволновый синтез наноразмерных материалов «ядро – оболочка» на основе магнетита, функционализированного золотом и доксорубицином. Российские нанотехнологии. 2017. 12(3–4):69–75.</mixed-citation></ref><ref id="B16"><label>16.</label><mixed-citation>Pryazhnikov D. V., Efanova O. O., Kiseleva M. S., Kubrakova I. V. Microwave synthesis of core–shell nanosize materials on the basis of magnetite functionalized with gold and doxorubicine. Nanotechnologies in Russia. 2017. 12(3–4):199.</mixed-citation></ref><ref id="B17"><label>17.</label><mixed-citation>Cao Z., Yue X., Li X., Dai Z. Stabilized Magnetic Cerasomes for Drug Delivery. Langmuir. 2013. 29:14976–14983.</mixed-citation></ref><ref id="B18"><label>18.</label><mixed-citation>Pryazhnikov D. V., Efanova O. O., Kubrakova I. V. Cerasomes containing magnetic nanoparticles: synthesis and gel-filtration chromatographic characterization. Mendeleev Commun. 2019. 29(2):226.</mixed-citation></ref><ref id="B19"><label>19.</label><mixed-citation>Dan Y., Zhang W., Xue R., Ma X., Stephan C., Shi H. Characterization of gold nanoparticle uptake by tomato plants using enzymatic extraction followed by single-particle inductively coupled plasma–mass spectrometry analysis. Environ. Sci. Technol. 2015. 49(5):3007.</mixed-citation></ref><ref id="B20"><label>20.</label><mixed-citation>Degueldre C., Favarger P.-Y. Colloid analysis by single particle inductively coupled plasma-mass spectroscopy: a feasibility study. Colloids Surf. A. 2003. 217:137.</mixed-citation></ref><ref id="B21"><label>21.</label><mixed-citation>Laborda F., Bolea E., Jiménez-Lamana J. Single particle inductively coupled plasma mass spectrometry for the analysis of inorganic engineered nanoparticles in environmental samples. Trends Environ. Anal. Chem. 2016. 9:15.</mixed-citation></ref><ref id="B22"><label>22.</label><mixed-citation>Temerdashev Z. A., Galitskaya O. A., Bolshov M. A. A novel method for the background signal correction in SP-ISP-MS analysis of the sizes of titanium dioxide nanoparticles in cosmetic samples. Molecules. 2022. 27. 7748.</mixed-citation></ref><ref id="B23"><label>23.</label><mixed-citation>Тимербаев А. Р. Роль масс-спектрометрии в разработке и внедрении в медицину металлсодержащих наночастиц. Журнал аналитической химии. 2015. 70(9):899–915.</mixed-citation></ref><ref id="B24"><label>24.</label><mixed-citation>Timerbaev A. R. Role of mass spectrometry in the development and medicinal implementation of metal-based nanoparticles. Journal of Analytical Chemistry. 2015. 70(9):1031.</mixed-citation></ref><ref id="B25"><label>25.</label><mixed-citation>Pitkänen L., Striegel A. M. Size-exclusion chromatography of metal nanoparticles and quantum dots. Trends Analyt. Chem. 2016. 80:311.</mixed-citation></ref><ref id="B26"><label>26.</label><mixed-citation>Катасонова О. Н., Федотов П. С. Методы проточного фракционирования микрочастиц: перспективы и области применения. Журнал аналитической химии. 2009. 64(3):228–242.</mixed-citation></ref><ref id="B27"><label>27.</label><mixed-citation>Katasonova O. N., Fedotov P. S. Methods for continuous flow fractionation of microparticles: Outlooks and fields of application. Journal of Analytical Chemistry. 2009. 64(3):212.</mixed-citation></ref><ref id="B28"><label>28.</label><mixed-citation>Mozhayeva D., Engelhard C. A critical review of single particle inductively coupled plasma mass spectrometry – A step towards an ideal method for nanomaterial characterization. J. Anal. At. Spectrom. 2020. 35: 1740–1783.</mixed-citation></ref></ref-list></back></article>
