Evolution of Macroscopic Properties of the System During Sol-Gel Synthesis of Lead Zirconate Titanate Ceramics Precursor

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Abstract

The influence of the amount of hydrolyzing agent on the kinetics of hydrolysis of lead zirconate-titanate precursor solution is considered from the point of view of the rate of change of hydrodynamic diameters of primary particles of the sol formed at the first stage, evolution of particle size distributions, rheological and optical properties of the colloidal systems. It is shown that changing the ratio of hydrolyzing agent: organometallic compounds is an effective controlling factor at the early stage of sol-gel-synthesis of piezoceramics of lead zirconate-titanate system and allows to obtain gel with controlled speed and necessary particle sizes.

About the authors

N. D. Paramonova

Joint Stock Company “Research Institute of Graphite-Based Structural Materials “NIIgraphite”; FGBOU VO “Mendeleev Russian Chemical Technology University”

Email: paramonova-nd@mail.ru
Moscow, Russia; Moscow, Russia

E. A. Danilov

Joint Stock Company “Research Institute of Graphite-Based Structural Materials “NIIgraphite”

Moscow, Russia

M. A. Vartanian

FGBOU VO “Mendeleev Russian Chemical Technology University”

Moscow, Russia

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