Observation of changes in the morphology of high-temperature metal films in a scanning probe microscope during warming up in open space conditions

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Abstract

Regularities of changes in the surface morphology of high-temperature metal coatings used as protective coatings can be applied to the structures of spacecraft sent closer to the Sun, have been observed. It is shown that films become less friable, and small grains of these films increase in size, as if spreading on the surface and rearranging into larger formations.

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About the authors

B. A. Loginov

National Research University of Electronic Technology MIET; Educational Centre "Sirius"

Author for correspondence.
Email: b-loginov@mail.ru
ORCID iD: 0000-0001-5081-1424
Russian Federation, Zelenograd; Sirius Federal Territory

Y. V. Khripunov

Educational Centre "Sirius"; Orel State University named after I.S.Turgenev

Email: b-loginov@mail.ru
ORCID iD: 0000-0003-2250-0420
Russian Federation, Sirius Federal Territory; Orel

M. A. Shcherbina

Educational Centre "Sirius"; Orel State University named after I.S.Turgenev

Email: b-loginov@mail.ru
ORCID iD: 0009-0001-8873-4986
Russian Federation, Sirius Federal Territory; Orel

A. O. Vyunik

Educational Centre "Sirius"

Email: b-loginov@mail.ru
ORCID iD: 0009-0000-8743-9013
Russian Federation, Sirius Federal Territory

V. D. Dmitrieva

Educational Centre "Sirius"

Email: b-loginov@mail.ru
ORCID iD: 0009-0009-8784-4815
Russian Federation, Sirius Federal Territory

A. A. Dyakova

Educational Centre "Sirius"

Email: b-loginov@mail.ru
ORCID iD: 0009-0009-8289-1065
Russian Federation, Sirius Federal Territory

M. K. Lebedeva

Educational Centre "Sirius"

Email: b-loginov@mail.ru
ORCID iD: 0009-0001-9070-3505
Russian Federation, Sirius Federal Territory

V. S. Makeev

Educational Centre "Sirius"

Email: b-loginov@mail.ru
ORCID iD: 0009-0009-3503-0078
Russian Federation, Sirius Federal Territory

A. R. Pervykh

Educational Centre "Sirius"

Email: b-loginov@mail.ru
ORCID iD: 0009-0008-8348-3111
Russian Federation, Sirius Federal Territory

D. S. Shevchenko

Educational Centre "Sirius"

Email: b-loginov@mail.ru
ORCID iD: 0009-0009-8866-0268
Russian Federation, Sirius Federal Territory

S. D. Khanin

Military Order of Zhukov and Lenin Red Banner Academy of Communications named after Marshal of the Soviet Union S.M. Budyonny of the Ministry of Defence of the Russian Federation

Email: b-loginov@mail.ru
ORCID iD: 0000-0002-8316-0362
Russian Federation, Saint-Petersburg

References

  1. Логинов Б.А. Первый в мире сканирующий зондовый микроскоп в виде спутника как старт этапа научных спутников-лабораторий. НАНОИНДУСТРИЯ, 2021. Т. 14. № 5. С. 22–26. https://doi.org/10.22184/1993-8578.2021.14.5.270.274
  2. Логинов Б.А. Комплекс зондовой микроскопии для работы в космическом пространстве и атмосфере. Патент на изобретение 2778278 C1, 17.08.2022, Заявка № 2021128836 от 04.10.2021.
  3. Электронный источник: Получены снимки с первого в мире спутникового сканирующего зондового микроскопа (дата обращения: 20.09.2023), ссылка: https://nauka.tass.ru/nauka/18422659
  4. Логинов Б.А., Логинов П.Б., Логинов В.Б., Логинов А.Б. Зондовая микроскопия: применения и рекомендации по разработке. НАНОИНДУСТРИЯ, 2019. Т. 12. № 6, C. 352–365. https://doi.org/10.22184/1993-8578.2019.12.6.366.369
  5. Loginov A.B., Ismagilov R.R., Obraztsov A.N., Bozhev I.V., Bokova-Sirosh S.N., Obraztsova E.D., Loginov B.A. Few-layer graphene formation by carbon deposition on polycrystalline Ni surface. Applied Surface Science, 2019. Vol. 494. PP. 1030–1035.
  6. Логинов А.Б., Божьев И.В., Бокова-Сирош С.Н., Образцова Е.Д., Исмагилов Р.Р., Логинов Б.А., Образцов А.Н. Формирование графена на поликристаллическом никеле. Журнал технической физики. 2019. Т. 89. № 11. PP. 1756–1762.
  7. Komarov N.S., Shevlyuga V.M., Loginov B.A., Andryushechkin B.V. Chlorine Adsorption on the Ag(110) Surface: STM and DFT Study". J. Phys. Chem. C. 2023. No. 127. PP. 2266−2273.
  8. Loginov A.B., Ismagilov R.R., Bokova-Sirosh S.N., Bozhev I.V., Obraztsova E.D., Loginov B.A., Obraztsov A.N. Formation of nanostructured films based on MoS2, WS2, MoO2 and their heterostructures. Technical Physics. Vol. 92. No. 13. P. 2078.
  9. Логинов Б.А., Хрипунов Ю.В., Щербина М.А., Вьюник А.О., Дмитриева В.Д., Дьякова А.А., Лебедева М.К., Макеев В.С., Первых А.Р., Шевченко Д.С., Ханин С.Д. Исследование способа термоэмиссионного распыления для создания тонкопленочных покрытий из металлов для работы сканирующего туннельного микроскопа в открытом космосе. НАНОИНДУСТРИЯ. 2024. Т. 17. № 1. С. 8–17. https://doi.org/10.22184/1993-8578.2024.17.1.8.17
  10. Логинов А.Б., Исмагилов Р.Р., Бокова-Сирош С.Н., Божьев И.В., Образцова Е.Д., Логинов Б.А., Образцов А.Н. Формирование наноструктурированных пленок MoS2, WS2, MoO2 и гетероструктур на их основе. Журнал технической физики. 2021. Vol. 91. No. 10. PP. 1509–1516.
  11. Loginov A.B., Fedotov P.V., Bokova-Sirosh S.N., Sapkov I.V., Chmelenin D.N., Ismagilov R.R., Obraztsova E.D., Loginov B.A., Obraztsov A.N. Synthesis, Structural, and Photoluminescence Properties of MoS2 Nanowall Films. Physica Status Solidi (B): Basic Research, John Wiley & Sons Ltd. (United Kingdom). 2022. PP. 2200481.
  12. Логинов А.Б., Бокова-Сирош С.Н., Федотов П.В., Сапков И.В., Хмеленин Д.Н., Исмагилов Р.Р., Образцова Е.Д., Логинов Б.А., Образцов А.Н. Получение и свойства мезопористых пленок MoS2". Физика и техника полупроводников. 2022. Vol. 56. No. 12. PP. 1112–1119.

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2. Fig.1. Diagrams and photos of sputtering and heating processes on the "MAG-5 vacuum-plasma unit": a – photo of sputtering process, b – photo of sputtering process, c – photo of heating process, d – photo of heating process; where: 1 – substrate, 2 – flying metal atoms, 3 – current-heated spiral from atomised metal, 4 – pumping and atmospheric inlet, 5 – current-heated tantalum strip, 6 – thermometer in the form of a spiral from bimetallic tape

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3. Fig.2. Operation of the "MAG-5A vacuum unit": a – in the process of sputtering; b – collective photo of all those who worked on the unit, from left to right: Maxim Shcherbina, Orel; Daria Shevchenko, Cherepovets; Victoria Dmitrieva, Orel; Anna Dyakova, Mezhdurechensk (Kuzbass); Vsevolod Makeev, Orel; Anton Pervykh, Orel; Yuri Khripunov, Orel; Boris Loginov, Zelenograd, Moscow; Alexei Vyunik, Volgograd; Maria Lebedeva, Biysk (Altai Territory)

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4. Fig.3. Characteristic 4 × 4 μm frames of surface morphology of sputtered (top) and further heated (bottom) films of different high-temperature metals (atomic number / melting point in degrees Celsius in brackets): a – vanadium (51/1910); b – tungsten (184/3422); c – hafnium (178/2227); d – molybdenum (96/2623); e – niobium (93/2477); f – zirconium (91/1855)

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5. Fig.4. Teams of schoolchildren at the Sirius Educational Centre in the project of the world’s first Earth probe microscope-satellite: a – the 2021 team, from left to right: Andrey Lopatin, Biysk, Altai Territory; Elizaveta Bespalova, Lipetsk; Alexander Vankaev, Astrakhan: Ekaterina Klyukina, Astrakhan; Mikhail Saprykin, Novosibirsk; Nikita Metalnikov, Orel; b – the 2022 team, left to right: Ekaterina Lyashko, Gatchina; Varvara Kirillova, Moscow; Anton Pervykh, Orel; Vsevolod Makeev, Orel; Vladislav Vtorova, Astrakhan; Danil Blinnikov, Orel

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Copyright (c) 2024 Loginov B.A., Khripunov Y.V., Shcherbina M.A., Vyunik A.O., Dmitrieva V.D., Dyakova A.A., Lebedeva M.K., Makeev V.S., Pervykh A.R., Shevchenko D.S., Khanin S.D.