LOW-TEMPERATURE SYNTHESIS OF HIGHLY DISPERSED BARIUM ALUMINATE

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Abstract

A new approach has been developed for the low-temperature synthesis of highly dispersed barium aluminate of vermicular morphology with specified characteristics (bulk density from 0.015 g/cm3, average particle size in the range of 15-87 nm). The synthesis technique includes sequential heat treatment up to 1200∘C of a concentrated aqueous solution of BaCl2, Al(NO3)3, (NH2)2CO and C6H8O7. Using physico-chemical research methods: IR spectroscopy, X-ray phase analysis, transmission and scanning electron microscopy, as well as chemical analysis, the main stages of the synthesis of BaAl2O4 are characterized.

About the authors

L. O. Kozlova

Kurnakov Institute of General and Inorganic Chemistry, Russian Academy of Sciences

Email: kozzllova167@gmail.com
Moscow, Russia

I. L. Voroshilov

Kurnakov Institute of General and Inorganic Chemistry, Russian Academy of Sciences

Moscow, Russia

Yu. V. Ioni

Kurnakov Institute of General and Inorganic Chemistry, Russian Academy of Sciences; Lomonosov Institute of Fine Chemical Technologies, MIREA—Russian Technological University

Moscow, Russia; Moscow, Russia

Yu. D. Ivakin

Moscow State University

Moscow, Russia

I. V. Kozerozhets

Kurnakov Institute of General and Inorganic Chemistry, Russian Academy of Sciences

Moscow, Russia

M. G. Vasiliev

Kurnakov Institute of General and Inorganic Chemistry, Russian Academy of Sciences

Moscow, Russia

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