Email this article Fabrication of a composite based on aluminum oxide nanofibers and nanodiamonds to construct phenol detection systems
- Authors: Ronzhin N.O.1, Posokhina E.D.1,2, Mikhlina E.V.3, Simunin M.M.2, Nemtsev I.V.4, Ryzhkov I.I.2,3, Bondar V.S.1
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Affiliations:
- Institute of Biophysics, Federal Research Center “Krasnoyarsk Scientific Center”, Siberian Branch of the Russian Academy of Sciences
- Siberian Federal University
- Institute of Computational Modeling, Federal Research Center “Krasnoyarsk Scientific Center”, Siberian Branch of the Russian Academy of Sciences
- Krasnoyarsk Science Centre of the Siberian Branch of Russian Academy of Science
- Issue: Vol 489, No 1 (2019)
- Pages: 44-48
- Section: Chemical Technology
- URL: https://journals.eco-vector.com/0869-5652/article/view/17862
- DOI: https://doi.org/10.31857/S0869-5652489144-48
- ID: 17862
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Abstract
A composite based on aluminum oxide nanofibers (AONF) and modified nanodiamonds (MND) synthesized by explosion technique was made by mixing aqueous suspensions of components at a 5:1 weight ratio and incubating the mixture for 15 minutes at 32 °C. It is assumed that the formation of a composite is provided by the difference in the zeta-potentials of the components - negative for MND and positive for AONF. Vacuum filtration of the mixture through a fluoroplastic filter (pore diameter of 0.6 µm) formed discs with a diameter of 40 mm with subsequent heat treatment at 300 °C to impart structural stability to the composite. Using scanning electron microscopy (SEM), it was revealed that the resulting composite has a network structure in which the MND particles are distributed over the AONF surface. It was established that MND incorporated into the composite catalyze the azo coupling reaction (phenol - 4-aminoantipyrine - H2O2) with the formation of a colored product (quinoneimine). The applicability of the composite for the multiple detection of phenol in aqueous samples is demonstrated.
Keywords
About the authors
N. O. Ronzhin
Institute of Biophysics, Federal Research Center “Krasnoyarsk Scientific Center”, Siberian Branch of the Russian Academy of Sciences
Author for correspondence.
Email: roniol@mail.ru
Russian Federation, 50, Akademgorodok, Krasnoyarsk, 660036
E. D. Posokhina
Institute of Biophysics, Federal Research Center “Krasnoyarsk Scientific Center”, Siberian Branch of the Russian Academy of Sciences; Siberian Federal University
Email: roniol@mail.ru
Russian Federation, 50, Akademgorodok, Krasnoyarsk, 660036; 79, Svobodny avenue, Krasnoyarsk, 660041
E. V. Mikhlina
Institute of Computational Modeling, Federal Research Center “Krasnoyarsk Scientific Center”, Siberian Branch of the Russian Academy of Sciences
Email: roniol@mail.ru
Russian Federation, 50/44, Akademgorodok, Krasnoyarsk, 660036
M. M. Simunin
Siberian Federal University
Email: roniol@mail.ru
Russian Federation, 79, Svobodny avenue, Krasnoyarsk, 660041
I. V. Nemtsev
Krasnoyarsk Science Centre of the Siberian Branch of Russian Academy of Science
Email: roniol@mail.ru
Russian Federation, 50, Akademgorodok, Krasnoyarsk, 660036
I. I. Ryzhkov
Siberian Federal University; Institute of Computational Modeling, Federal Research Center “Krasnoyarsk Scientific Center”, Siberian Branch of the Russian Academy of Sciences
Email: roniol@mail.ru
Russian Federation, 79, Svobodny avenue, Krasnoyarsk, 660041; 50/44, Akademgorodok, Krasnoyarsk, 660036
V. S. Bondar
Institute of Biophysics, Federal Research Center “Krasnoyarsk Scientific Center”, Siberian Branch of the Russian Academy of Sciences
Email: roniol@mail.ru
Russian Federation, 50, Akademgorodok, Krasnoyarsk, 660036
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