Analytical Сontrol of Raw Materials and Products in Metallurgy Based on the Use of Certified Reference Materials

Cover Page

Full Text

Open Access Open Access
Restricted Access Access granted
Restricted Access Subscription or Fee Access

Abstract

The Institute for Certified Reference Materials has developed and approved accuracy standards that define uniform metrological requirements for measurement techniques (methods) and reference materials (RM). Certified Reference Materials (CRM) produced by ICRM correspond in matrix to real materials of metallurgical production. Based on the use of matrix CRM and accuracy standards, a system of metrological support for analytical control of metallurgical materials has been created, including validation of measurement technique (methods), operational and in-laboratory control of results, certification of enterprise RM, interlaboratory comparison tests, etc.

Full Text

Restricted Access

About the authors

Valery V. Stepanovskikh

Institute for Certified Reference Materials

Author for correspondence.
Email: v.stepanovskikh@icrm-ekb.ru
ORCID iD: 0009-0004-5729-8837

Candidate of Technical Sciences, Director

Russian Federation, Ekaterinburg

Elena K. Kolpakova

Institute for Certified Reference Materials

Email: e.kolpakova@icrm-ekb.ru

Head of the Center for Preparation and Certification of Certified Reference Materials

Russian Federation, Ekaterinburg

Rashida K. Khuzagaleeva

Institute for Certified Reference Materials

Email: mle@icrm-ekb.ru

Head of the Quality Service of Reference Materials of the CPC

Russian Federation, Ekaterinburg

References

  1. On reference materials for chemical analysis of products of metallurgical industry enterprises: Resolution of the Economic Council under the Council of People’s Commissars of the USSR of April 3, 1939, No. 290 [in Russ.].
  2. Komar N. P. Chemical metrology, its past, present and future. Izvestiya vuz. Chemistry and chemical technology. 1975; 18(3), 343–355 [in Russ.].
  3. Shaevich A. B. Measurement and regulation of chemical composition. Moscow: Izdatel’stvo standartov Publ., 1971. 280 p. [in Russ.].
  4. Püschel R. Zum Problem der „Genauigkeit“ chemischer Analysen. Mikrochimica Acta. 1968. 56(4): 783–801.
  5. Pliner Yu.L., Svechnikova E. A., Ogurtsov V. M. Quality management of chemical analysis in metallurgy. Moscow: Izdatel’stvo Metallurgija Publ.,1979. 208 p. [in Russ.].
  6. Pliner Yu.L., Kuzmin I. M. Metrological problems of analytical quality control of metal products. Moscow: Izdatel’stvo Metallurgija Publ.,1989. 216 p. [in Russ.].
  7. Pliner Yu.L., Kuzmin I. M., Pyrina M. P., Stepanovskikh V. V. Accuracy of analytical control of ferrous metals. Moscow: Izdatel’stvo Metallurgija Publ., 1994. 256 p. [in Russ.].
  8. MU MO 14-1-61-90. Guidelines. Accuracy Standards for Quantitative Chemical Analysis of Ferrous Metallurgy Materials. Sverdlovsk: ISO TsNIIChM Publ., 1990. 19 p. [in Russ.].
  9. MU MO 14-1-3-90. Certification of Non-Standardized Methods of Quantitative Chemical Analysis. Sverdlovsk: ISO TsNIIChM Publ., 1990. 24 p. [in Russ.].
  10. MU MO 14-1-4-90. Development and Approval of Standard Samples of Enterprises. Sverdlovsk: ISO TsNIIChM Publ., 1990. 44 p. [in Russ.].
  11. MU MO 14-1-6-90. Metrological Expertise of Draft Standards for Ferrous Metallurgy Materials and Methods of Their Quantitative Chemical Analysis. Sverdlovsk: ISO TsNIIChM Publ., 1990. 8 p. [in Russ.].
  12. MU MO 14-1-9-90. Statistical quality control of analytical laboratories of ferrous metallurgy enterprises and organizations. Sverdlovsk: ISO TsNIIChM Publ., 1990. 12 p. [in Russ.].
  13. M 11-90. Methodology for Control of Chemical Reagents Based on the Use of Standard Samples. Sverdlovsk, 1990. 7 p. [in Russ.].
  14. M 20-2010. Recommendation. Accuracy Standards for Quantitative Chemical Analysis of Ferrous Metallurgy Materials. Yekaterinburg: ZAO Institute of Standard Samples Publ., 2010. 37 p. (With Amendment No. 1 of 24.02.2014) [in Russ.].
  15. GOST R 54569-2011. Cast Iron, Steel, Ferroalloys, Metallic Chromium and Manganese. Accuracy Standards for Quantitative Chemical Analysis. Moscow: Standartinform Publ., 2012. 16 p. [in Russ.]

Supplementary files

Supplementary Files
Action
1. JATS XML

Copyright (c) 2024 Stepanovskikh V.V., Kolpakova E.K., Khuzagaleeva R.K.