Determination of residual organic solvents in 2-benzoylamino-n-[4-(4,6-dimethylpyrimidin-2- ylsulfamoil)-phenyl]-benzamide by gas chromatography
- Authors: Borovskiy B.V1, Koval’ N.O1, Kompancev V.A1, Kodonidi I.P1, Larskiy M.V1, Rasskazov A.G1
-
Affiliations:
- Pyatigorsk Medical and Pharmaceutical Institute - branch of Volgograd State Medical University
- Issue: Vol 24, No 4 (2021)
- Pages: 15-23
- Section: Articles
- URL: https://journals.eco-vector.com/1560-9596/article/view/112838
- DOI: https://doi.org/10.29296/25877313-2021-04-03
- ID: 112838
Cite item
Abstract
Full Text
About the authors
B. V Borovskiy
Pyatigorsk Medical and Pharmaceutical Institute - branch of Volgograd State Medical University
Email: b.v.borovskiy@pmedpharm.ru
Ph.D (Pharm.), Associate Professor, Department of Inorganic, Physical and Colloid Chemistry Pyatigorsk, Russia
N. O Koval’
Pyatigorsk Medical and Pharmaceutical Institute - branch of Volgograd State Medical UniversityPost-graduate Student, Department of Inorganic, Physical and Colloid Chemistry Pyatigorsk, Russia
V. A Kompancev
Pyatigorsk Medical and Pharmaceutical Institute - branch of Volgograd State Medical UniversityDr.Sc. (Pharm.), Professor, Department of Inorganic, Physical and Colloid Chemistry Pyatigorsk, Russia
I. P Kodonidi
Pyatigorsk Medical and Pharmaceutical Institute - branch of Volgograd State Medical UniversityDr.Sc. (Pharm.), Professor, Department of Organic Chemistry Pyatigorsk, Russia
M. V Larskiy
Pyatigorsk Medical and Pharmaceutical Institute - branch of Volgograd State Medical University
Email: m.v.larsky@pmedpharm.ru
Ph.D (Pharm.), Associate Professor, Head of the Department of Pharmaceutical Chemistry Pyatigorsk, Russia
A. G Rasskazov
Pyatigorsk Medical and Pharmaceutical Institute - branch of Volgograd State Medical UniversityLecturer, Department of Toxicological and Analytical Chemistry Pyatigorsk, Russia
References
- Александровский Ю.А., Этиологические факторы и механизмы формирования невротических расстройств. Психиатрия: национальное руководство. М.: ГЭОТАР-Медиа, 2011. С. 25-30.
- Полищук Ю.И., Летникова З.В.Многофакторные причины возникновения и развития непсихотических депрессивных и тревожных расстройств в позднем возрасте. Социальная и клиническая психиатрия.2019; 29(2): 86-92.
- Патент РФ № 2643356. Новое N-арилсульфамидное производное о-бензоиламинобензойной кислоты, обладающее анксиолитической, актропротекторной и антидепрессивной активностью. Э.Т. Оганесян, И.П. Кодониди, Э.А. Манвелян, В.С. Сочнее, В.Ю. Сыса, М.М. Манвелян. 2018.
- Yang G., Jahan M.S., Ahsan L., Zhang L.Q., Ni Y.H. Rapid determination of formic and acetic acids in biomass hydrolysate by headspace gas chromatography. Bioresour Technol. 2013; 138: 258.
- Zhao G.H., Nyman M., Jonsson J.A. Rapid determination of short-chain fatty acids in colonic contents and faeces of humans and rats by acidified water-extraction and direct-injection gas chromatography. Biomed. Chromatography. 2006; 20(8): 674-682.
- Torii T., Kanemitsu K., Wada T., Itoh S., Kinugawa K., Hagiwara A. Measurement of short-chain fatty acids in human faeces using high-performance liquid chromatography: specimen stability. Ann. Clin. Biochem. 2010; 47(5): 447-452.
- Ferreir F.N., Carneiro M.C., Vaitsman D.S., Pontes F.V.M., Monteiro M.I.C., Da Silva L.I.D., Neto A.A. Matrix-elimination with steam distillation for determination of short-chain fatty acids in hypersaline waters from pre-salt layer by ion-exclusion chromatography. J. Chromatography A. 2012; 1223: 79-83.
- Hey T., Sandstrom D., Ibrahim V., Jonsson K. Evaluating 5 and 8 pH-point titrations for measuring VFA in full-scale primary sludge hydrolysate. Water SA 2013; 39(1): 17-22.
- Dandan Z., Qingxi H., Wei L., Xiaoli R. Rapid determination of formic and acetic acids in biomass hydrolysate by headspace gas chromatography. Journal of Industrial and Engineering Chemistry. 2017; 47: 281-287.
- Blau K., Halket J. (Eds.) Handbook of Derivatisation for Chromatography, 2nd ed. Heyden, London. 1993.
- Wells R.J. Recent advances in non-silylation derivatization techniques for gas chromatography. J. Chromatography A. 1999; 843(1-2): 1-18.
- Husek P. Chloroformates in gas chromatography as general purpose derivatizing agents. J. Chromatography B. 1998; 717(1-2): 57-91.
- Wittmann Gy., Van Langenhove H., Dewulf J. Determination of acetic acid in aqueous samples, by water-phase derivatisation, solid-phase microextraction and gas chromatography. Journal of Chromatography A. 2000; 874(2): 225-234.
- Keerthi K., Valli Kumari R. V., Tulja Rani G. Head space gas chromatography analysis of residual solvents in temozolomide by using Zb-624 Column. International Journal of Research Studies in Biosciences (IJRSB). 2015; 3(6): 92-100.
- Вигдергауз М.С. Расчеты в газовой хроматографии. М.: Химия, 1978. 248 с.
- Витенберг А.Г., Конопелько Л.А. Парофазный газохроматографический анализ: метрологические приложения. Журнал аналитической химии. 2011; 66(5): 452-472.
- Руководство ICN «Валидация аналитических методик». Содержание и методология. Фармация. 2008; 4: 3-10.