The method of mass spectrometry with matrix/nanosurface assisted laser desorption/ionization
- Authors: Krasnova T.A1, Amelin V.G1
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- Issue: No 10 (2013)
- Pages: 34-36
- Section: Articles
- URL: https://journals.eco-vector.com/1019-8946/article/view/327585
- ID: 327585
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Abstract
The new rapid procedure identifying 31 antibiotic residues by mass spectrometry with matrix /nanosurface - assisted laser desorption / ionization (MALDI / NALDI MS) in milk was developed. As a matrix α-cyano-4-hydroxycinnamic acid and standard substrates nanosurface of the company Bruker Daltonic («Nanosys MSP 96») were used. To remove antibiotics from milk ace-tonitrile was applied without subsequent purification of the extract. Limits of detection were 0.001-0.3 mg/kg, the duration of the analysis is 20-30 min.
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References
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